前言
Preface
第1章 仪器分析实验基本知识
Chapter 1 Basic Knowledge of Instrumental Analysis Experiments
1.1 仪器分析实验要求
1.1 Requirements for Instrumental Analysis
1.2 仪器分析实验安全知识
1.2 Safety Knowledge of Instrumental Analysis
1.3 仪器分析实验数据记录与处理
1.3 Record and Treatment of Instrumental Analysis Experimental Data
1.4 仪器分析实验室用水
1.4 Water Used in Analytical Laboratories
1.5 仪器分析样品前处理技术
1.5 Pretreatment Techniques for Instrumental Analysis of Samples
第2章 验证性仪器分析实验
Chapter 2 Confirmatory Instrumental Analysis Experiments
2.1 氟离子选择电极测定饮用水中的氟
2.1 Determination of Fluoride Ions in Drinking Water by Fluoride Ion Selective Electrode
2.2 醋酸电位滴定
2.2 Potentiometric Titration of Acetic Acid
2.3 邻二氮菲分光光度法测定水中微量铁
2.3 Spectrophotometric Determination of Trace Iron in Water by 1.0 Phen.anthroline
2.4 喹啉的荧光特性和含量测定
2.4 Fluorescence Properties and Content Determination of Quinoline
2.5 阿司匹林红外吸收光谱的测定
2.5 Determination of Infrared Absorption Spectrum of Aspirin
2.6 原子吸收法测定感冒冲剂中的铜
2.6 Determination of Copper in Cold Granules by Atomic Absorption Spectrometry
2.7 核磁共振氢谱法确定有机化合物的分子结构
2.7 Identification of the Molecular Structure of Organic Compounds by H-NMR Spectroscopy
2.8 薄层色谱法鉴别复方磺胺甲嗯唑片
2.8 Identification of Compound Sulfamethoxazole Tablets by Thin Layer Chromatography
2.9 纸色谱法分离氨基酸
2.9 Separation of Amino Acids by Paper Chromatography
2.10 气相色谱仪性能考察
2.10 Performance Examination of the Gas Chromatograph System
2.11 高效液相色谱仪基本操作与系统适应性
2.11 Basic Operation and System Adaptability of High.performance Liquid Chromatography
2.12 高效液相色谱法定性分析
2.12 Qualitative Analysis by High Performance Liquid Chromatography
2.13 毛细管区带电泳分离手性药物的对映异构体
2.13 Separation of Enantiomers of Chiral Drugs by Capillary Zone Electrophoresis
第3章 综合性仪器分析实验
Chapter 3 Comprehensive Instrumental Analysis Experiments
3.1 循环伏安法检测对乙酰氨基酚
3.1 Detection of Acetaminophen by Cyclic Voltammetry Method
3.2 双波长等吸收点法测定速洁舒洗剂中醋酸氯己定的含量
3.2 Content Determination of Chorhexidine Acetate in SuJie Shu Detergent by Dual.wavelength Isoabsorption Point Method
3.3 安钠咖注射液中苯甲酸钠和咖啡因的含量测定
3.3 Content Determination of Sodium Benzoate and Caffeine in Caffeine and Sodium Benzoate Injection
3.4 气相色谱法测定祛伤消肿酊中樟脑、薄荷脑和龙脑的含量
3.4 Content Determination of Camphor，Menthol and Borneol in Qushang Xiaozhong Tincture by Gas Chromatography
3.5 高效液相色谱法三种定量分析方法测定苯的含量
3.5 Content Determination of Benzene by Three Quantitative Analysis Methods in High Performance Liquid Chromatography
3.6 高效液相色谱一质谱联用法鉴定双黄连口服液中的有效成分
3.6 Identification of Active Components in Shuang-huanglian Oral Liquid by High Performance Liquid ChrOmatography-Mass Spectrometry
第4章 设计性仪器分析实验
Chapter 4 Designed Instrumental Analysis Experiments
4.1 中药胆矾中CuSO2的含量测定
4.1 Content Determination of CuS04 in the Traditional Chinese Medicine Bile Alum
4.2 药物的有关物质检查实验
4.2 Related Substance Tests of Drugs
4.3 中药制剂的含量测定
4.3 Content Determination of Chinese Medicine Preparation
附录
附录1 821型离子计的操作规程
附录2 pHS3-C(A)型精密酸度计操作规程
附录3 UVl000紫外-可见分光光度计操作规程
附录4 CAAM.2001原子吸收光谱仪操作规程
附录5 岛津IR Affinity-1型傅里叶红外光谱仪的操作规程
附录6 岛津GC-2014气相色谱仪的操作规程
附录7 普析LC-600高效液相色谱仪操作步骤
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